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CERTIFICATE OF ANALYSIS
Product name Fish collagen Hydrolyzed Use description food
Raw material Fish skin Batch No 20130625
Manufactured Date 20130625 Expiry date 20160624
Serial No. Items of Inspect Specification Inspection Result Test Methods
1 Appearance White flowing powder pass Visual
2 Odor None or few special odor pass Organoleptic
3 Protein% ≥90 91.65 USP 34
4 pH（1% water solution） 5.0-7.5 6.30 6.67%,45℃
5 Ash % ≤2.0 0.60 Residue On Ignition,17h,550℃
6 Moisture% ≤8.0 3.60 17h,105℃
7 Molecular Weight( Da) 1000-2000 pass HPSEC
8 Grain Size (g/cm3) 0.1-0.4 0.25 Graduated Cylinder
9 Lead（Pb） (mg/kg) ≤5.0 ＜5.0 AAS
10 As (mg/kg) ≤1.0 ＜1.0 Atomic Absorption Spectroscopy AAS
11 SO2 (mg/kg) ≤50 10.2 USP 32
12 Total Bacteria (cfu/g) ≤1000 202 According to GME
13 Total Coliforms (MPN/100g) ≤30 pass According to GME
14 Total Saccharomycete (cfu/g) ≤25 pass According to GME
15 Mold count(cfu/g) ≤25 pass According to GME
16 Pathogenic bacteria ( Salmonella sp., Staphylococcus aureus ) Negative pass
According to GME
17 Conclusion pass
Storage: Store in a cool dry area. Keep away from strong light and heat.
Shelf light: 3 years when properly stored.
------------------------------------------------------------------------------------------------------------------------------------------CONCLUSION: CONFORM TO THE REQUIREMENTS.
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Checker: 03 Analyst: 05